Answer :
Solution :
The reasons for the melting point determines :
- the assignment of the sample's purity
- identification of the unknown sample
- the conversion of solid sample to the liquid completely
In order to prepare the sample in the capillary tube for determining its melting point, we tap the tube gently into the sample with the open end of tube down. We then continue tapping the tube till the sample is couple of millimeters high.
Then the other close end of tube down, we tap the sample down again slowly or then dropping the tube into a longer tube so as to move down the sample faster.